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  • 1.
    Biswas, Tuser
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Functionalization of textiles with enzymes by inkjet printing2018Conference paper (Refereed)
    Abstract [en]

    The catalytic activity of the enzymes can be introduced to textile surfaces for bio-sensing applications by immobilizing them through a resource-efficient deposition method such as inkjet printing [1]. Contrary to conventional dispensing methods, drop-on-demand inkjet printing can provide with high precision deposition of these enzymes along with flexibility for small-scale production [2]. To the best of our knowledge, studies on the inkjetting of enzymes are limited and often uses a modified/adapted commercial paper printer for jetting [3]. Additionally, the effect of ink formulation and printing condition variables on the activity of enzyme are not well explored. Many of such variables suggested for jetting of proteins [4] includes e.g. ink rheology, operating temperature, drop size retention, and the shear force acting on the ink. In our research effect of these variables are studied using a digital inkjet printer (Xennia Carnelian) with a Sapphire QS10 piezo-electric print head (Fujifilm Dimatix, USA). Lysozyme is used as a model enzyme for printing due to its well-known structure and catalytic mechanism. Effect of temperature and shear force development within the print head on lysozyme activity is investigated. Additionally, pre-treatment of the fabric to improve ink adhesion through various surface activation processes are studied. Finally, remaining activity of the printed enzymes over washing is evaluated to ensure the fastness property.

    Acknowledgment

    This research project is funded by University of Borås, Sweden.

    References

    [1]     Li J, Rossignol F, Macdonald J. Inkjet printing for biosensor fabrication: combining chemistry and technology for advanced manufacturing. Lab on a Chip 2015;15(12):2538-2558.

    [2]     Nierstrasz V, Yu J, Seipel S. Towards more flexible, sustainable and energy-efficient textile functionalization processes: Digital inkjet in functional and smart textile production. In: 9th Aachen-Dresden International Textile Conference 2015; 2015.

    [3]     Yamazoe H. Fabrication of protein micropatterns using a functional substrate with convertible protein-adsorption surface properties. J Biomed Mater Res A 2012;100(2):362-9.

    [4]     Delaney JT, Smith PJ, Schubert US. Inkjet printing of proteins. Soft Matter 2009;5(24):4866-4877.

  • 2.
    Biswas, Tuser
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Inkjetting of Enzymes: Chapter 122019In: Advance in Textile Biotechnology 2nd edition / [ed] Artur Cavaco-Paulo, Vincent Nierstrasz, Qiang Wang, Elsevier, 2019Chapter in book (Refereed)
  • 3.
    Nechyporchuk, Oleksandr
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Bordes, Romain
    Cellulose Nanofibril-Based Coatings of Woven Cotton Fabrics for Improved Inkjet Printing with a Potential in E-Textile Manufacturing2017In: ACS Sustainable Chemistry & Engineering, E-ISSN 2168-0485Article in journal (Refereed)
    Abstract [en]

    The inherent flammability of cellulosic fibers limits their use in some advanced applications. This work demonstrates for the first time the production of flame-retardant macroscopic fibers from wood-derived cellulose nanofibrils (CNF) and silica nanoparticles (SNP). The fibers are made by extrusion of aqueous suspensions of anionic CNF into a coagulation bath of cationic SNP at an acidic pH. As a result, the fibers with a CNF core and a SNP thin shell are produced through interfacial complexation. Silica-modified nanocellulose fibers with a diameter of ca. 15 μm, a titer of ca. 3 dtex and a tenacity of ca. 13 cN tex–1 are shown. The flame retardancy of the fibers is demonstrated, which is attributed to the capacity of SNP to promote char forming and heat insulation on the fiber surface.

  • 4.
    Nierstrasz, Vincent
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Seipel, Sina
    University of Borås, Faculty of Textiles, Engineering and Business.
    Digital inkjet in functional and smart textile production: turning wet textile processes into dry and energy-efficient processes.2015In: Proceedings of the 54th Dornbirn Man-Made Fibre Congres, 16-18 September 2015, Dornbirn, Austria., 2015, p. 1-18Conference paper (Refereed)
    Abstract [en]

    Conventional textile dyeing and finishing processes typically utilize large quantities of water, energy and chemicals. Despite many efforts to improve resource efficiency textile industry still needs to find radical solutions to substantially reduce its ecological footprint. The objective of the research is to enable textile industry to introduce more effective processes avoiding unnecessary use of water, energy, chemicals and minimization of waste.Digital inkjet technology is a technology with large potential in resource effective production of high end products such as functional and smart textiles in addition to colour printing on textiles. Moreover, digital inkjet technology stimulates innovation through the possibility of small batches, enables novel production strategies (digitalisation of the value chain) and it effectively bridges design and technology. The technology offers strong potential in made-to-measure smart textiles with e.g. applications in health-care and sports.Our research projects in digital inkjet technology focus on the development of stable functional inks, in order to produce textiles with e.g. superhydrophobic, antistatic, conductive, UV sensing or antimicrobial properties as well as inks for color printing.

  • 5.
    Nierstrasz, Vincent
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Seipel, Sina
    University of Borås, Faculty of Textiles, Engineering and Business.
    Towards more flexible, sustainable and energy-efficient textile functionalization processes: Digital inkjet in functional and smart textile production2015Conference paper (Other academic)
    Abstract [en]

    Conventional textile processes are characterized by large scale production runs and typically utilize large quantities of water, energy and chemicals, making them less suitable for the production of functional and smart textiles. Key objective of the research initiative is to introduce flexible, more resource effective textile functionalization processes.

    Digital inkjet technology is a technology with large potential in resource effective production of high end products such as functional and smart textiles in addition to colour printing on textiles. The challenge is to make the potential of digital inkjet technology in high end products an opportunity for the European textile industry.

    Digital inkjet technology stimulates innovation through the possibility of small production runs, enables novel production strategies (digitalisation of the value chain) and it effectively bridges design and technology. The technology offers strong potential in made-to-measure smart textiles with e.g. applications in health-care and sports.

  • 6.
    Nierstrasz, Vincent
    et al.
    University of Borås, Swedish School of Textiles.
    Yu, Junchun
    University of Borås, Swedish School of Textiles.
    Seipel, Sina
    University of Borås, Swedish School of Textiles.
    Agnhage, Tove
    University of Borås, Swedish School of Textiles.
    Functionalization of textile materials using inkjet technology2014In: 53rd DORNBIRN MAN-MADE FIBERS CONGRESS, Dornbirn MFC , 2014, Vol. 60911PM1330, p. 1-8Conference paper (Other academic)
  • 7.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Junchun, Yu
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Sustainable production of a UV-sensing smart textile2015Conference paper (Other academic)
    Abstract [en]

    The general objective of our research is to develop smart textiles using novel production techniques like digital inkjet printing. Digital inkjet printing enables a sustainable and integrated textile production where less energy, water and chemicals are used, as well as less waste is produced. Inkjet printing can typically be used for the production of small batches, which benefits the production of technical and smart high end products. The advantage compared to traditional textile production techniques is that functionalizing chemicals are applied only where needed and complex designs can easily be changed.

    Smart textiles are capable of interacting with the environment and are therewith ideal, flexible lightweight sensors [1]. A wearable and integrated sensor technology can among others be developed through the functionalization of textiles with chromic materials. By showing a reversible colour change a photochromic textile can make the user aware of an environmental danger such as augmented UV-radiation coupled with certain temperature conditions [2,3].

    Our research focus on the sustainable production of a UV-sensing smart textile leads to the exploration of minimized water and energy consumption in textile production. In specific, a radiation curable matrix as carrier for the functional material is investigated. The challenge in our work is to consider the role of radiation as curer and activator, as well as the effect of temperature in order to optimize the functionality range of the sensor. Furthermore, storage tests of photochromic prints are conducted to determine the storage stability of the UV-sensor. 

  • 8.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Viková, Martina
    Technical University of Liberec.
    Vik, Michal
    Technical University of Liberec.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Inkjet printing and UV-LED curing of photochromic dyes for functional and smart textile applications2018In: RSC Advances, ISSN 2046-2069, E-ISSN 2046-2069, Vol. 8, no 50, p. 28395-28404Article in journal (Refereed)
    Abstract [en]

    Health concerns as a result of harmful UV-rays drive the development of UV-sensors of different kinds. In this research, a UV-responsive smart textile is produced by inkjet printing and UV-LED curing of a specifically designed photochromic ink on PET fabric. This paper focuses on tuning and characterizing the colour performance of a photochromic dye embedded in a UV-curable ink resin. The influence of industrial fabrication parameters on the crosslinking density of the UV-resin and hence on the colour kinetics is investigated. A lower crosslinking density of the UV-resin increases the kinetic switching speed of the photochromic dye molecules upon isomerization. By introducing an extended kinetic model, which defines rate constants kcolouration, kdecayand kdecolouration, the colour performance of photochromic textiles can be predicted. Fabrication parameters present a flexible and fast alternative to polymer conjugation to control kinetics of photochromic dyes in a resin. In particular, industrial fabrication parameters during printing and curing of the photochromic ink are used to set the colour yield, colouration/decolouration rates and the durability, which are important characteristics towards the development of a UV-sensor for smart textile applications.

  • 9.
    Seipel, Sina
    et al.
    University of Borås, Swedish School of Textiles.
    Yu, Junchun
    University of Borås, Swedish School of Textiles.
    Nierstrasz, Vincent
    University of Borås, Swedish School of Textiles.
    Development of a Textile UV-Sensor2014Conference paper (Other academic)
  • 10.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, JunchunUniversity of Borås, Faculty of Textiles, Engineering and Business.Nierstrasz, VincentUniversity of Borås, Faculty of Textiles, Engineering and Business.
    Digital inkjet printing as flexible and resource-saving production technique for a smart textile UV-sensor2016Conference proceedings (editor) (Other academic)
  • 11.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Digital inkjet printing as flexible and resource-saving production technique for a smart textile UV-sensor2016Conference paper (Other academic)
  • 12.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Production of a UV-curable and UV-sensing smart textile using digital inkjet printing2016In: Books of abstracts: Aachen-Dresden-Denkendorf International Textile Conference, Dresden, 2016Conference paper (Other academic)
  • 13.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Periyasamy, Aravin
    Technical University of Liberec.
    Viková, Martina
    Technical University of Liberec.
    Vik, Michal
    Technical University of Liberec.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Characterization and optimization of an inkjet-printed smart textile UV-sensor cured with UV-LED light2017In: IOP Conference Series: Materials Science and Engineering, 2017, Vol. 254, article id 072023Conference paper (Refereed)
    Abstract [en]

    For the development of niche products like smart textiles and other functional high-end products, resource-saving production processes are needed. Niche products only require small batches, which makes their production with traditional textile production techniques time-consuming and costly. To achieve a profitable production, as well as to further foster innovation, flexible and integrated production techniques are a requirement. Both digital inkjet printing and UV-light curing contribute to a flexible, resource-efficient, energy-saving and therewith economic production of smart textiles. In this article, a smart textile UV-sensor is printed using a piezoelectric drop-on-demand printhead and cured with a UV-LED lamp. The UVcurable ink system is based on free radical polymerization and the integrated UVsensing material is a photochromic dye, Reversacol Ruby Red. The combination of two photoactive compounds, for which UV-light is both the curer and the activator, challenges two processes: polymer crosslinking of the resin and color performance of the photochromic dye. Differential scanning calorimetry (DSC) is used to characterize the curing efficiency of the prints. Color measurements are made to determine the influence of degree of polymer crosslinking on the developed color intensities, as well as coloration and decoloration rates of the photochromic prints. Optimized functionality of the textile UV-sensor is found using different belt speeds and lamp intensities during the curing process.

  • 14.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Periyasamy, Aravin
    Technical University of Liberec.
    Viková, Martina
    Technical University of Liberec.
    Vik, Michal
    Technical University of Liberec.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Resource-Efficient Production of a Smart Textile UV Sensor Using Photochromic Dyes: Characterization and Optimization2018In: Narrow and Smart Textiles / [ed] Prof. Dr. Yordan Kyosev, Prof. Dr. Boris Mahltig, Prof. Dr. Anne Schwarz-Pfeiffer, Springer Publishing Company, 2018, p. 251-257Chapter in book (Refereed)
  • 15.
    Seipel, Sina
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Viková, Martina
    Technical University of Liberec.
    Vik, Michal
    Technical University of Liberec.
    Koldinská, Marie
    Technical University of Liberec.
    Havelka, Antonin
    Technical University of Liberec.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Color performance, durability and handle of inkjet-printed and UV-cured photochromic textiles for multi-colored applications2019In: Fibers And Polymers, ISSN 1229-9197, E-ISSN 1875-0052, Vol. 20Article in journal (Refereed)
    Abstract [en]

    The development and design of novel functional and smart textile materials such as textile sensors and multicolored systems based on photochromic dyes necessitate controls of color intensities, switching speeds, and material durability. Precise control and synchronization of dye kinetics are important for multi-colored photochromic applications especially. However, durability towards abrasion and washing should not be compromised on if we aim to design reliable future textile products. In this study, two different commercial photochromic dyes — a naphthopyran and a spirooxazine-based dye — have been applied on PET fabric by inkjet printing and UV-LED curing. The photochromic textiles’ color behavior, fastness to abrasion and washing, and handle are evaluated using spectrophotometry, scanning electron microscopy, and Kawabata evaluation system. Despite a decrease in color performance after washing, the photochromic inkjet print is effective and barely influences the textile structure. Reduced rigidity of the host matrix promoted higher color yields and faster dye kinetics, but also improved durability towards abrasion and washing. In order to synchronize kinetics of the different dye types for multi-colored applications, distinct curing conditions are preferable, which, however, result in varying print durability. In the design of multi-colored photochromic textiles, dye kinetics, and durability have to be balanced.

  • 16.
    Tadesse, Melkie Getnet
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Effect of chemical concentration on the rheology of inkjet conductive inks2018Conference paper (Refereed)
    Abstract [en]

    Viscosity and surface tension are the fundamental rheological property of an ink for inkjet printing. In this work, we optimized the viscosity and surface tension of inkjet inks by varying the concentration of glycerol with water, PEDOT-PSS with glycerol and water, finally by adding the surfactant. The surface resistance of the sample was characterized by four-probe measurement principle. The change in volume of PEDOT-PSS in water, as well as the change in weight of glycerol in water has got a great influence on the viscosity on both temperature dependence and shear dependence behaviour of the ink solution. The surface tension of the solution changed from 37 to 28mN/m due to the addition of Triton. Varying the volume of PEDOT-PSS and the volume of glycerol in water has a great influence on the viscosity of the ink solution for inkjet printing. Viscosity drops from 12.5 to 9.5 mPa s with the addition of Triton at 25 oC. The PEDOT-PSS solution was found to be temperature dependence but not shear dependence as it is a Newtonian fluid. The sample was used to connect the light emitting diode (LED), and hence the electrical conductivity, with a surface resistance of 0.158 KΩ/square, was sufficient enough to give transfer current for LED lamp. The rheology of the inkjet ink is very critical for the successful droplet formation of the inkjet printing.

  • 17.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Digital inkjet functionalization of water-repellent textile for smart textile application2018In: Journal of Materials Science, ISSN 0022-2461, E-ISSN 1573-4803Article in journal (Refereed)
    Abstract [en]

    Digital inkjet printing is a production technology with high potential in resource efficient processes, which features both flexibility and productivity. In this research, waterborne, fluorocarbon-free ink containing polysiloxane in the form of micro-emulsion is formulated for the application of water-repellent sports- and work wear. The physicochemical properties of the ink such as surface tension, rheological properties and particle size are characterized, and thereafter inkjet printed as solid square pattern (10 × 10 cm) on polyester and polyamide 66 fabrics. The water contact angle (WCA) of the functional surfaces is increased from < 90° to ca. 140° after 10 inkjet printing passes. Moreover, the functional surface shows resistance to wash and abrasion. The WCA of functional surfaces is between 130° and 140° after 10 wash cycles, and is ca. 140° after 20000 revolutions of rubbing. The differences in construction of the textile as well as ink–filament interaction attribute to the different transportation behaviors of the ink on the textile, reflected in the durability of the functional layer on the textile. The functionalized textile preserves its key textile feature such as softness and breathability. Inkjet printing shows large potential in high-end applications such as customized functionalization of textiles in the domain of smart textiles.

  • 18.
    Yu, Junchun
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business. vincent.nierstrasz@hb.se.
    Seipel, Sina
    University of Borås, Faculty of Textiles, Engineering and Business.
    Inkjet printing of waterborne hydrophobic ink for functionalization of textile2015Conference paper (Other academic)
    Abstract [en]

    Digital inkjet printing of functional layer on textiles is a resource efficient and flexible manufacturing process, with reduced ecological footprint. This technology has large potential in high-end applications such as in the domain of smart textiles. The purpose of our research is to develop a waterborne, fluorocarbon free ink for water-repellent sports- and work- wear. The novel ink formulation was characterized by measuring surface tension and rheology and thereafter inkjet printed as solid block pattern (10×10 cm) on polyester fabrics. The hydrophobicity of the functional surface was characterized by water contact angle measurements. The wash fastness and abrasion properties of functional surface were investigated. The inkjet printed functional surface shows promising hydrophobicity compared to commercial available products.

  • 19.
    Yu, Junchun
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Seipel, Sina
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    DEVELOPMENT OF HYDROPHOBIC INK FOR INKJET PRINTING OF FUNCTIONAL TEXTILE2016Conference paper (Other academic)
    Abstract [en]

    Digital inkjet printing is a resource effective and flexible manufacturing method, which has great potential to replace the large-scale conventional textile processes, and stimulates innovation in small and flexible production such as in the domain of smart textiles. Water-repellent textile has great importance in the application of sport- and work- wear. In this research, a hydrophobic ink free from fluorocarbon is formulated. The rheological properties, surface tension and particle size were characterized in order to fit the jetting parameter of the print head. In order to improve the adhesion between the deposited ink and substrate, plasma and alkaline pre-treatment were performed on polyester substrate. The novel formulation was inkjet printed as the solid bock on polyester and polyamide 6,6. The hydrophobicity of the fabrics was measured by water contract angle measurement. The effect of pre-treatment on the adhesion of ink to substrate as well as on functional property of textile was evaluated after washing and abrasion tests.   

  • 20.
    Yu, Junchun
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Seipel, Sina
    University of Borås, Faculty of Textiles, Engineering and Business.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Inkjet printing of functional ink for smart textile application2016Conference paper (Other academic)
    Abstract [en]

    Fluorocarbon-free, water-repellent inks for sports- and work- wear were developed and inkjet printed. The inkjet printed samples show promising hydrophobicity and fastness properties. The result indicates that it can be possible to combine inkjet printing and functional ink as resource efficient production method for customization in the domain of smart textile.

  • 21.
    Zhou, Yuyang
    et al.
    University of Borås, Faculty of Textiles, Engineering and Business.
    Yu, Junchun
    University of Borås, Faculty of Textiles, Engineering and Business.
    Biswas, Tuser
    University of Borås, Faculty of Textiles, Engineering and Business.
    Tang, Ren-Cheng
    National Engineering Laboratory for Modern Silk, College of Textile and Clothing Engineering, Soochow University, 199 Renai Road, Suzhou 215123, China.
    Nierstrasz, Vincent
    University of Borås, Faculty of Textiles, Engineering and Business.
    Inkjet Printing of Curcumin-Based Ink for Coloration and Bioactivation of Polyamide, Silk, and Wool Fabrics2019In: ACS Sustainable Chemistry & Engineering, E-ISSN 2168-0485, Vol. 7, no 2Article in journal (Refereed)
1 - 21 of 21
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