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Fungi-Based Biorefinery: Valorization of industrial residuals and techno-economic evaluation
University of Borås, Faculty of Textiles, Engineering and Business.
2022 (English)Doctoral thesis, comprehensive summary (Other academic)
Sustainable development
According to the author(s), the content of this publication falls within the area of sustainable development.
Abstract [en]

Sustainable development of society and industry is necessary for a safer future that is being challenged by environmental pollution, climate change, and scarcity of food and nutrition. Materials considered as waste can be converted into value-added products and energy, hence regained to the economy. Filamentous fungi are saprophytic microorganisms that show great potential for bioconversion of organic waste materials into a wide range of products, including ethanol, enzymes, fungal biomass, and organic acids. In this study, industrial residuals from bioethanol plants (thin stillage), agro-industrial residuals (oat husks), and fruit-processing residuals were considered as potential substrates for filamentous fungi. Different filamentous fungi species were investigated due to their edibility and ability to produce ethanol. The aim of this study was to investigate 1) the feasibility of a biorefinery concept and contribution of fungal products to the process economy, 2) the valorization of oat husks in the fungal biorefinery and its contribution to the process economy, and 3) the effect of bioactive compounds existing in fruit residuals on filamentous fungi in a synthetic medium.

Bioconversion of thin stillage into value-added products, e.g., additional ethanol produced by filamentous fungi and edible fungal biomass for various feed/food markets, improved the process economy of a conventional bioethanol plant. Techno-economic analysis was carried out with Aspen Plus® and Aspen Process Economic Analyzer®. The economy of the conventional bioethanol plant was improved to 76% and 5.6-fold higher net present value when the fungal product was sold as fish feed and human food, respectively. When the fungal product was sold as human food, Aspergillus oryzae was more advantageous than Neurospora intermedia. It is possible to integrate lignocellulosic material into the fungi-based biorefinery and produce additional products, e.g., lignin and fungal biomass as feed/food products. Several scenarios for integrating organosolv pretreatment into the biorefinery were investigated. When protein-rich biomass was sold as feed and food, 71% and 7.9-fold higher net present value was obtained, respectively, compared to the conventional ethanol plant. Similarly, other materials, e.g., fruit residuals, can be valorized through the fungal biorefinery. However, bioactive compounds in fruit residuals have antimicrobial effects; therefore, it is essential to assess the sensitivity of fungi toward them for efficient processes. In addition to the fungi species utilized in thin stillage and oat husk valorization, two other industrially important fungi, Rhizopus oligosporus and A. niger, were tested against 10 bioactive compounds with antimicrobial properties (octanol, ellagic acid, (-)-epicatechin, quercetin, betanin, ascorbic acid, limonene, hexanal, car-3-ene, and myrcene). The bioactive compounds were added to a synthetic medium to reach final concentrations of 2.4, 24 and 240 mg/L, within their natural concentration in fruit/fruit residuals. A. oryzae, A. niger and N. intermedia were inhibited by octanol, while the latter fungus was also inhibited by D-Limonene at 240 mg/L. On the other hand, R. oligosporus was resistant to inhibitory compounds and increased the biomass yield. The highest change in biomass yield was in the presence of ellagic acid with up to a 4-fold increase. Ethanol and lactic acid yields were increased 38% and 30% in the presence of ellagic acid and betanin, respectively. Similarly, the existence of quercetin and ellagic acid, ascorbic acid, and hexanal increased the biomass yield of A. niger up to 28%.

These studies can contribute to developing efficient and feasible biorefineries, in which filamentous fungi convert the industrial residuals into value-added products.

Place, publisher, year, edition, pages
Borås: Högskolan i Borås, 2022.
Series
Skrifter från Högskolan i Borås, ISSN 0280-381X ; 130
Keywords [en]
Techno-economic analysis, Organosolv, bioethanol, filamentous fungi, food, lignin, fruit, bioactive compounds
National Category
Environmental Biotechnology
Research subject
Resource Recovery
Identifiers
URN: urn:nbn:se:hb:diva-28588ISBN: 978-91-89271-78-4 (print)ISBN: 978-91-89271-79-1 (electronic)OAI: oai:DiVA.org:hb-28588DiVA, id: diva2:1695425
Public defence
2022-11-18, C203, Allégatan 1, Borås, 10:09 (English)
Opponent
Supervisors
Available from: 2022-10-28 Created: 2022-09-13 Last updated: 2022-10-27Bibliographically approved
List of papers
1. Techno-Economic Analysis of Bioethanol Plant By-Product Valorization: Exploring Market Opportunities with Protein-Rich Fungal Biomass Production
Open this publication in new window or tab >>Techno-Economic Analysis of Bioethanol Plant By-Product Valorization: Exploring Market Opportunities with Protein-Rich Fungal Biomass Production
2020 (English)In: Fermentation, E-ISSN 2311-5637, Vol. 6, no 4Article in journal (Refereed) Published
Abstract [en]

The feasibility of dry-grind bioethanol plants is extremely dependent on selling prices of ethanol and by-products, known as Dried distillers grains with solubles (DDGS), and sold as animal feed. Increasing the amount and quality of the by-products can widen potential feed and food markets and improve the process economy and robustness to price fluctuations of ethanol and grain. In this study, the techno-economic analysis of a bioethanol plant was investigated. Integration of edible filamentous fungi into the process leading to the conversion of sidestreams into ethanol and protein-rich fungal biomass for food and feed applications was considered, and its impact was investigated. Sensitivity analysis considered variations on process capacity, on the price of grain and ethanol, and on the price of fungal biomass considering its use for various animal feed (e.g., pig and fish) and human food markets. Selling the fungal biomass in the human food market resulted in 5.56 times higher NPV (net present value) than the base case bioethanol plant after 20 years. Integration of a low-performing strain towards ethanol, followed by the usage of the fungal biomass in the food sector, was found to be the most resistant scenario to the low ethanol selling price and increasing grain price. This study showed that the competitiveness of ethanol plants in the fuel market could be reinforced while meeting the increasing demand for protein sources.

Place, publisher, year, edition, pages
MDPI, 2020
Keywords
bioethanol process, grains, filamentous fungi, feed, food, thin stillage
National Category
Industrial Biotechnology
Identifiers
urn:nbn:se:hb:diva-24794 (URN)10.3390/fermentation6040099 (DOI)000601569600001 ()2-s2.0-85107550562 (Scopus ID)
Available from: 2021-01-25 Created: 2021-01-25 Last updated: 2022-10-27Bibliographically approved
2. Retrofitting analysis of a biorefinery: Integration of 1st and 2nd generation ethanol through organosolv pretreatment of oat husks and fungal cultivation
Open this publication in new window or tab >>Retrofitting analysis of a biorefinery: Integration of 1st and 2nd generation ethanol through organosolv pretreatment of oat husks and fungal cultivation
2021 (English)In: Bioresource Technology Reports, E-ISSN 2589-014X, Vol. 15, article id 100762Article in journal (Refereed) Published
Abstract [en]

This study was dedicated to techno-economic analysis of an integrated 1st and 2nd generation biorefinery, where the organosolv pretreated oat husk and thin stillage is valorized through filamentous fungi and baker yeast. By this strategy, process economy can benefit from multiple value-added products including lignin (80% purity), and protein-rich biomass as feed/food ingredients. Ethanol recovery of organosolv pretreatment benefits the already existing equipment in 1st generation ethanol plant. The best results shows that the integration of 10 tons/h oat husk into a process using 18.8 tons/h grains results in increasing ethanol production from 5.2 to 7.5 tons/h, in addition to 1.6 tons/h lignin (80% purity) and 7.6 tons/h fungal biomass. Integrated process is beneficial not only for 2nd but also for 1st generation ethanol production. Selling the fungal biomass as feed and food increased the net present value (NPV) in comparison to conventional ethanol plant by 71% and 7.9-fold, respectively. © 2021 The Authors

Place, publisher, year, edition, pages
Elsevier Ltd, 2021
Keywords
Ethanol, Filamentous fungi, Lignin, Organosolv, Pretreatment, Techno-economic analysis, Biomass, Economic analysis, Fungi, Refining, Ethanol plants, Ethanol production, Fungal biomass, Organosolv pretreatment, The net present value (NPV), Value added products, Bioethanol, alcohol, arabinoxylan, food ingredient, glucan, hexose, lignocellulose, pentose, solvent, starch, xylan, alcohol production, Article, ash, biomass valorization, biorefinery, economic aspect, fermentation, filamentous fungus, fungal strain, fungus, growth, industry, moisture, Neurospora intermedia, nonhuman, oat, oat husk, process development, Saccharomyces cerevisiae, sensitivity analysis, sustainable development
National Category
Biochemistry and Molecular Biology
Research subject
Resource Recovery
Identifiers
urn:nbn:se:hb:diva-26908 (URN)10.1016/j.biteb.2021.100762 (DOI)2-s2.0-85109884931 (Scopus ID)
Funder
Swedish Agency for Economic and Regional Growth
Note

Export Date: 17 November 2021; Article; Correspondence Address: Bulkan, G.; Swedish Centre for Resource Recovery, Sweden; email: gulru.bulkan@hb.se

Available from: 2021-11-17 Created: 2021-11-17 Last updated: 2024-08-30Bibliographically approved
3. Enhancing or inhibitory effect of fruit or vegetable bioactive compound on Aspergillus niger and A. oryzae
Open this publication in new window or tab >>Enhancing or inhibitory effect of fruit or vegetable bioactive compound on Aspergillus niger and A. oryzae
Show others...
2022 (English)In: Journal of Fungi, E-ISSN 2309-608X, Vol. 8, no 1, article id 12Article in journal (Refereed) Published
Abstract [en]

Fruit and vegetable processing wastes are global challenges but also suitable sources with a variety of nutrients for different fermentative products using bacteria, yeast or fungi. The interaction of microorganisms with bioactive compounds in fruit waste can have inhibitory or enhancing effect on microbial growth. In this study, the antimicrobial effect of 10 bioactive compounds, including octanol, ellagic acid, (−)-epicatechin, quercetin, betanin, ascorbic acid, limonene, hexanal, car-3-ene, and myrcene in the range of 0–240 mg/L on filamentous fungi Aspergillus oryzae and Aspergillus niger were investigated. These fungi were both found to be resistant to all compounds except octanol, which can be used as a natural antifungal agent, specifically against A. oryzae and A. niger contamination. On the contrary, polyphenols (quercetin and ellagic acid), ascorbic acid, and hexanal enhanced A. niger biomass yield 28%, 7.8%, 16%, and 6%, respectively. Furthermore, 240 mg/L car-3-ene was found to increase A. oryzae biomass yield 8%, while a 9% decrease was observed at lower concentration, 24 mg/L. Similarly, up to 17% decrease of biomass yield was observed from betanin and myrcene. The resistant nature of the fungi against FPW bioactive compounds shows the potential of these fungi for further application in waste valorization. © 2021 by the authors. Licensee MDPI, Basel, Switzerland.

Place, publisher, year, edition, pages
MDPI, 2022
Keywords
Aspergillus, Bioactive, Filamentous fungi, Flavor, Fruit processing waste, Inhibitor
National Category
Other Industrial Biotechnology
Research subject
Resource Recovery
Identifiers
urn:nbn:se:hb:diva-27168 (URN)10.3390/jof8010012 (DOI)000747433700001 ()2-s2.0-85121801445 (Scopus ID)
Funder
Swedish Agency for Economic and Regional Growth, 20201656
Available from: 2022-01-11 Created: 2022-01-11 Last updated: 2024-08-30Bibliographically approved
4. Inhibitory and Stimulatory Effects of Fruit Bioactive Compounds on Edible Filamentous Fungi: Potential for Innovative Food Applications
Open this publication in new window or tab >>Inhibitory and Stimulatory Effects of Fruit Bioactive Compounds on Edible Filamentous Fungi: Potential for Innovative Food Applications
Show others...
2022 (English)In: Fermentation, E-ISSN 2311-5637, Vol. 8, no 6, article id 270Article in journal (Refereed) Published
Abstract [en]

The fermentation of fruit processing residuals (FPRs) with filamentous fungi can provide protein-rich food products. However, FPRs that contain bioactive compounds with antimicrobial properties present a major challenge. In this work, the resistance of two edible filamentous fungi, Rhizopus oligosporus and Neurospora intermedia, to 10 typically inhibiting bioactive compounds available in FPRs (epicatechin, quercetin, ellagic acid, betanin, octanol, hexanal, D-limonene, myrcene, car-3-ene, and ascorbic acid) was examined. These compounds’ inhibitory and stimulatory effects on fungal growth were examined individually. Three different concentrations (2.4, 24, and 240 mg/L) within the natural concentration range of these compounds in FPRs were tested. These bioactive compounds stimulated the growth yield and glucose consumption rate of R. oligosporus, while there was no increase in the biomass yield of N. intermedia. Ellagic acid caused an up to four-fold increase in the biomass yield of R. oligosporus. In addition, octanol and D-limonene showed antifungal effects against N. intermedia. These results may be helpful in the development of fungus-based novel fermented foods. View Full-Text

Place, publisher, year, edition, pages
MDPI, 2022
Keywords
filamentous fungi, Rhizopus oligosporus, Neurospora intermedia, fruit, bioactive compound, food, inhibitor
National Category
Microbiology
Identifiers
urn:nbn:se:hb:diva-28756 (URN)10.3390/fermentation8060270 (DOI)000816636900001 ()2-s2.0-85132163459 (Scopus ID)
Funder
Swedish Agency for Economic and Regional Growth
Available from: 2022-10-17 Created: 2022-10-17 Last updated: 2022-10-28

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